NFT 30-077

Kesternich testing simulates acid rain or industrial chemical exposure  to evaluate the relative corrosion resistance of the coating, substrate, or part itself.  Parts or panels are placed inside a specially designed chamber and are exposed to SO2  and humidity before being evaluated for resistance to corrosion.  The following standard used in this type of test.

NFT 30-077 Test Standard specifies a method for determining the resistance of a paint film, paint systems and related products to conditions of high humidity. The method is applicable to coatings both on porous substrates, such as wood, plaster and plasterboard, as well as on non-porous substrates, such as metal. It gives an indication of the performance likely to be obtained under severe exposure conditions and when continuous condensation occurs on the surface. The procedure may show coating defects (including blistering, staining, softening, crimping, embrittlement) and deterioration of the substrate. It also determines Ash Content.

ISO 11503

Kesternich testing simulates acid rain or industrial chemical exposure  to evaluate the relative corrosion resistance of the coating, substrate, or part itself.  Parts or panels are placed inside a specially designed chamber and are exposed to SO2  and humidity before being evaluated for resistance to corrosion.  The following standard used in this type of test.

ISO 11503 Test Standard deals with the testing of paints, varnishes and related products. Specifies a test method for determining under standard conditions the resistance of a single coat or a multi-coat system of paint or related material in intermittent water condensation.

IEC 60068-2-52 – Methods 1-6

IEC 60068-2-52

Test specimens are placed in an enclosed chamber (a separate salt mist chamber and controlled humidity chamber are generally used) and exposed to a changing climate that starts with 2 hours exposure to a continuous indirect spray of neutral (pH 6.5 to 7.2) salt water solution, which falls-out on to the specimens at a rate of 1.0 to 2.0ml/80cm²/hour, in a chamber temperature of +15 to +35°C.  Depending upon method number, this is followed either by exposure to a high humidity climate of 40°C / 93%RH; or air drying at 60 °C, under 30 % RH and then Wetting at 50°C.

The proven test methodolgy can be downloaded here

The duration of high humidity and number of cycle repeats is variable depending on the test method (1-8).

Test method 1

One cycle consists of spraying samples with salt solution at 35 °C for 2h, followed by controlled humidity at 40 °C, 93% RH for six days and 22 h. The required number of cycles is four (28 days).

Test method 2

One cycle consists of spraying samples with salt solution at 35 °C for 2h, followed by controlled humidity at 40 °C, 93% RH for 22h. The required number of cycles is three (3 days).

Test method 3

One cycle consists of spraying samples with a salt solution at 35 °C for 2h, followed by controlled humidity at 40 °C, 93% RH for 22h. This shall be repeated four times. The test specimens shall then be stored under standard atmosphere at 23 °C and 50 % RH for three days. The required number of cycles is one (seven days).

Test method 4

The required number of cycles as specified in test method 3 shall be two (14 days).

Test method 5

The required number of cycles as specified in test method 3 shall be four (28 days).

Test method 6

The required number of cycles as specified in test method 3 shall be eight (56 days).

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IEC 60068-2-52 – Methods 7-8

ISO 60068-2-52

Test specimens are placed in an enclosed chamber (a separate salt mist chamber and controlled humidity chamber are generally used) and exposed to a changing climate that starts with 2 hours exposure to a continuous indirect spray of neutral (pH 6.5 to 7.2) salt water solution, which falls-out on to the specimens at a rate of 1.0 to 2.0ml/80cm²/hour, in a chamber temperature of +15 to +35°C.  Depending upon method number, this is followed either by exposure to a high humidity climate of 40°, C93%RH; or air drying at 60 °C, under 30 % RH and then Wetting at 50°C.

The duration of high humidity and number of cycle repeats is variable depending on the test method (1-8).

Test method 7

One cycle is 8 h. One cycle shall consist of spraying the specimen with salt solution at 35 °C for 2 h, followed by the dry condition at 60 °C, under 30 % RH for 4 h and then the humid condition at 50 °C, over 95 % RH for 2 h.

The transition times (time allowed to reach the temperature and relative humidity specified for a condition after changing to that condition) for temperature and humidity shall be specified between the following choices and reported: – salt mist to dry condition: within 30 min or between 30 min and 60 min; – dry condition to humid condition: within 15 min or between 15 min and 30 min; – humid condition to salt mist: within 30 min. Those transition times shall be included in the next condition period of the pair, for example the salt mist to dry condition transition time is included in the period of the dry condition. Spraying the specimen with a salt solution begins instantaneously once the salt mist is started.

The recommended number of cycles are 3 (1 day), 6 (2 days), 12 (4 days), 30 (10 days), 45 (15 days), 60 (20 days), 90 (30 days), 150 (50 days) and 180 (60 days).

Test method 8

One cycle is 8 h, as specified in test method 7 using acidified salt solution instead of neutral salt solution.

The recommended number of cycles is the same as in test method 7

EN 13523-8

Salt spray corrosion tests in artificial atmospheres

EN 13523-8 can be used to test the relative resistance to corrosion of metallic materials with or without temporary or permanent corrosion protection, when exposed to a salt spray climate (neutral salt spray or acetic acid salt spray or copper accelerated acetic acid salt spray) at an elevated temperature.

Test specimens are placed in an enclosed chamber and exposed to a continuous indirect spray of neutral (pH 6.5 to 7.2) or acidified (pH3.1 to 3.3) salt water solution, which falls-out on to the specimens at a rate of 1.0 to 2.0ml/80cm²/hour, in a chamber temperature of +35C. This climate is maintained under constant steady state conditions. The test duration is variable.

EN 13523-8 tests are also referred to as a NSS, ASS & CASS tests.

For further information on EN 13523-8

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LV124

In recent years the automotive industry has been faced with many technical challenges in attempting to comply with a series of industrial norms. One of the most important of these norms is LV 124, which was jointly developed by a group of German automobile manufacturers; Daimler Benz, Audi, BMW, Volkswagen, and Porsche.

Most of these manufacturers have now developed their own version of this standard, these include Mercedes (MBN LV 124-1), BMW(GS 95024-2-1), and VW (VW 80000).

This complex 160 page standard covers test procedures for electrical and electronic components in passenger motor vehicles weighing less than 3.5 tonnes, and includes electrical tests, mechanical tests, climatic tests, and service life tests.

Amongst the many individual tests within the standard is a requirement for corrosion testing, this element of LV 124 is based upon EN 60068-2-11, which is undertaken to test the resistance of the component to malfunction when exposed to a salt spray climate at an elevated temperature, due to short circuits and leakage currents caused by ingress of salt into the component.

ISO14993

Corrosion of Metals & Alloys – accelerated testing involving cyclic exposure to salt mist, dry & wet conditions

This test method specifies the apparatus and procedure to be used in conducting accelerated corrosion tests for the comparative evaluation of metallic materials, with or without permanent/temporary corrosion protection, when exposed to a salt contaminated, simulated outdoor environment. It is cyclic in nature, i.e.; test specimens are exposed to changing climates over time.

Test specimens are placed in an enclosed chamber and exposed to a changing climate that comprises of the following 3 part repeating cycle. 2.0 hours exposure to a continuous indirect spray of neutral (pH 6.5 to 7.2) salt water solution, which falls-out on to the specimens at a rate of 1.0 to 2.0ml/80cm²/hour, in a chamber temperature of +35C . This is followed by 4.0 hours of air drying in a climate of <30%RH at +60C. This is followed by 2.0 hours exposure to a condensing water climate (wetting) of 95 to 100%RH at +50C. The number of cycle repeats and therefore the test duration is variable.

The maximum transition times between each part of the test cycle are also specified as follows:

From salt spraying to air drying within 30 minutes.

From air drying to wetting within 15 minutes.

From wetting to salt spraying within 30 minutes.

Chamber volumes of less than 400 Litres are not permitted by this test standard.

This test is also referred to as a Cyclic Corrosion Test, often abbreviated to CCT., and is the international version of JASO M609/M610/CCT-1

For further information on ISO standards visit; www.iso.org

Note; many ISO test standards have been harmonized with other European standards and these are now prefixed ‘EN’ (Euro Norm) or ‘** EN’ – where ** are the letters representing a European country/language code, for example ‘BS EN’ for a harmonized British standard in English language.

ISO 16701

Accelerated corrosion test involving exposure under controlled conditions of humidity and intermittent spraying of salt solution

Accelerated corrosion tests to simulate atmospheric corrosion in such environments include cyclic exposure to a wet phase, during which the test object is repeatedly subjected first to a spray of salt solution then to a wet stand-by period for several hours. This is followed by a phase of controlled cyclic humidity conditions, where the test object is subjected to an environment which alternates between high humidity and comparative dryness.

In the first (wet) phase of exposure, the test objects are sprayed for 15 min with a 1% (mass fraction) aqueous solution of sodium chloride acidified to pH 4.2, to simulate the rather acidic precipitation present in industrialized areas, followed by a 1 h 45 min period of wet stand-by. This sequence is repeated three times to give a total of 6 h exposure to wetness. The whole of this first phase of the test cycle is repeated twice a week.

The major part of the test cycle, however, consists of humidity cycling between the two levels of 95 % RH and 50 % RH at a constant temperature of 35°C.

This test is also referred to as a Cyclic Corrosion Test, often abbreviated to CCT.

ISO11997-Cycle B

Paints & varnishes – determination of resistance to cyclic corrosion conditions, Part 1: wet(salt fog)/dry/humidity

This test method has been found to be useful for comparing the relative resistance to corrosion of paints, varnishes and similar materials, when exposed to a simulated aggressive outdoor environment, such as a marine environment. It is cyclic in nature, i.e.; test specimens are exposed to changing climates over time.

3 different test cycles are defined within this test method, which are referred to as Cycle A, Cycle B & Cycle C.

Cycle A is based upon test CCT-4. Please see elsewhere in this document for details of CCT-4. This test method has been shown to correlate well with natural exposure for thermosetting paints. The number of cycle repeats is to be sufficient for 1000 hours total test time, unless otherwise agreed.

Cycle B is based upon test VDA 621-415. Please see elsewhere in this document for details of VDA 621-415. This test method has been shown to correlate well with natural exposure for thermosetting paints in vehicle corrosion. The number of cycle repeats is to be sufficient for 840 hours total test time, unless otherwise agreed.

Cycle C has been developed in the UK for use with water soluble and latex paint systems, and has been shown to correlate well with natural exposure. Cycle C test specimens are placed in an enclosed chamber and exposed to a changing climate that comprises of the following repeating cycle. 210 minutes exposure hours exposure to a continuous indirect spray of salt water solution, which falls-out on to the specimens at a rate of 2.0 to 4.0ml/80cm²/hour, in a chamber temperature of +25C. This is followed by 210 minutes exposure to an air drying climate at +40C (humidity unspecified). This is followed by 1470 minutes exposure to a controlled humidity climate of 75%RH at +40C. This is followed by 102 minutes exposure to an air drying climate at +25C (humidity unspecified). This is followed by 210 minutes exposure to a salt fog climate at +25C. This is followed by 378 minutes exposure to a condensing water climate of 95 to 100%RH at +30C. This is followed by 180 minutes exposure to an air drying climate at +35C (humidity unspecified). This is followed by 120 minutes exposure to an air drying climate at +25C (humidity unspecified). The number of cycle repeats is to be sufficient for 1000 hours total test time, unless otherwise agreed.

Chamber volumes of less than 400 Litres are not permitted by this test standard.

These tests are also referred to as a Cyclic Corrosion Tests, often abbreviated to CCT.

For further information on ISO standards visit; www.iso.org

Note; many ISO test standards have been harmonized with other European standards and these are now prefixed ‘EN’ (Euro Norm) or ‘** EN’ – where ** are the letters representing a European country/language code, for example ‘BS EN’ for a harmonized British standard in English language.

ISO11997-Cycle A

Paints & varnishes – determination of resistance to cyclic corrosion conditions, Part 1: wet(salt fog)/dry/humidity

This test method has been found to be useful for comparing the relative resistance to corrosion of paints, varnishes and similar materials, when exposed to a simulated aggressive outdoor environment, such as a marine environment. It is cyclic in nature, i.e.; test specimens are exposed to changing climates over time.

3 different test cycles are defined within this test method, which are referred to as Cycle A, Cycle B & Cycle C.

Cycle A is based upon test CCT-4. Please see elsewhere in this document for details of CCT-4. This test method has been shown to correlate well with natural exposure for thermosetting paints. The number of cycle repeats is to be sufficient for 1000 hours total test time, unless otherwise agreed.

Cycle B is based upon test VDA 621-415. Please see elsewhere in this document for details of VDA 621-415. This test method has been shown to correlate well with natural exposure for thermosetting paints in vehicle corrosion. The number of cycle repeats is to be sufficient for 840 hours total test time, unless otherwise agreed.

Cycle C has been developed in the UK for use with water soluble and latex paint systems, and has been shown to correlate well with natural exposure. Cycle C test specimens are placed in an enclosed chamber and exposed to a changing climate that comprises of the following repeating cycle. 210 minutes exposure hours exposure to a continuous indirect spray of salt water solution, which falls-out on to the specimens at a rate of 2.0 to 4.0ml/80cm²/hour, in a chamber temperature of +25C. This is followed by 210 minutes exposure to an air drying climate at +40C (humidity unspecified). This is followed by 1470 minutes exposure to a controlled humidity climate of 75%RH at +40C. This is followed by 102 minutes exposure to an air drying climate at +25C (humidity unspecified). This is followed by 210 minutes exposure to a salt fog climate at +25C. This is followed by 378 minutes exposure to a condensing water climate of 95 to 100%RH at +30C. This is followed by 180 minutes exposure to an air drying climate at +35C (humidity unspecified). This is followed by 120 minutes exposure to an air drying climate at +25C (humidity unspecified). The number of cycle repeats is to be sufficient for 1000 hours total test time, unless otherwise agreed.

Chamber volumes of less than 400 Litres are not permitted by this test standard.

These tests are also referred to as a Cyclic Corrosion Tests, often abbreviated to CCT.

For further information on ISO standards visit; www.iso.org

Note; many ISO test standards have been harmonized with other European standards and these are now prefixed ‘EN’ (Euro Norm) or ‘** EN’ – where ** are the letters representing a European country/language code, for example ‘BS EN’ for a harmonized British standard in English language.